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Reviewed CSCA Chemistry question · Standard

A mixture contains solid iodine and solid potassium iodide. Iodine is slightly soluble in water, while potassium iodide is very soluble. Which method is most appropriate to separate and purify the iodine?

  1. Add water, filter, and evaporate the filtrate
  2. Add water, filter, and dry the residue
  3. Heat the mixture to sublime the iodine and collect it on a cold surface
  4. Dissolve in ethanol, then evaporate the solvent
Show the answer and explanation

Correct answer

C. Heat the mixture to sublime the iodine and collect it on a cold surface

Principle or equation

Iodine sublimes when heated, changing directly from solid to gas, while potassium iodide does not sublime. Sublimation can separate a sublimable solid from a non-sublimable one.

Why this answer is correct

Heating the mixture causes iodine to sublime; the purple vapor can be condensed on a cold surface, leaving potassium iodide behind. This is a direct and efficient method. Adding water would dissolve potassium iodide and also some iodine, making separation less effective. Ethanol would dissolve both, not separating them.

Example

I2(s) → I2(g) → I2(s) (on cold surface)

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